The mol-ecular structure from the title compound C28H20N4O6 includes three fused six-membered rings (a methyl-ene unit. × 0.11 mm Data collection Bruker APEXII CCD diffractometer Absorption correction: multi-scan (> 2σ(= 1.00 4828 reflections 343 guidelines H-atom guidelines constrained Δρmax = 0.12 e ??3 Δρmin = ?0.15 e ??3 Data collection: (Bruker 2009 ?); cell refinement: (Bruker 2009 ?); data decrease: (Sheldrick 2008 ?); system(s) utilized to refine framework: (Sheldrick 2008 ?); molecular images: (Farrugia 1997 ?); software program used to get ready materials for publication: = 508.48= 10.0780 (3) ?Cell guidelines from 7395 reflections= 22.7094 (6) ?θ = 2.4-21.5°= 11.2729 (3) ?μ = 0.10 mm?1β = 113.809 (1)°= 296 K= 2360.41 (11) ?3Prism yellow= 40.40 × 0.14 × 0.11 mm Notice in another windowpane Data collection Bruker APEXII CCD diffractometer4828 individual reflectionsRadiation resource: fine-focus sealed pipe2998 reflections with > 2σ(= ?12→12= ?28→2847772 measured reflections= ?12→14 Notice in another windowpane Refinement Refinement on = 1.00= GRLF1 1/[σ2(= (and goodness of in shape derive from derive from collection to zero for adverse F2. The threshold manifestation Iressa of F2 > 2 can be used only for determining R-elements(gt) etc. and isn’t relevant to the decision of reflections for refinement. R-elements predicated on F2 are statistically about doubly huge as those predicated on F and R– elements predicated on ALL data will become even larger. Notice in another windowpane Fractional atomic coordinates and comparative or isotropic isotropic displacement guidelines (?2) xconzUiso*/UeqC10.6321 Iressa (2)0.82375 (9)0.19097 (19)0.0612 (5)C20.85135 (19)0.84194 (8)0.35084 (17)0.0552 (4)C30.81023 (17)0.89317 (8)0.27367 (15)0.0502 (4)C40.90411 (17)0.94182 (7)0.30538 (15)0.0475 (4)C51.04177 (18)0.93398 (7)0.40936 (15)0.0505 (4)C61.0776 (2)0.88249 (8)0.48157 (16)0.0593 (5)H61.16830.87940.54980.071*C70.9829 (2)0.83582 (8)0.45530 (17)0.0622 (5)H71.00640.80180.50550.075*C81.1555 (2)0.97997 (8)0.44241 (17)0.0574 (4)C91.1231 (2)1.03401 (8)0.36364 (17)0.0556 (4)C100.98508 (19)1.04342 (7)0.26723 (16)0.0527 (4)C110.86591 (19)1.00068 (8)0.24546 (16)0.0524 (4)C121.2303 (2)1.07627 (9)0.3858 (2)0.0712 (5)H121.32241.07030.45050.085*C131.2012 (3)1.12668 (10)0.3127 (2)0.0793 (6)H131.27301.15500.32920.095*C141.0663 (3)1.13554 (9)0.2151 (2)0.0754 (6)H141.04821.16920.16410.090*C150.9574 (2)1.09440 (8)0.19255 (19)0.0651 (5)H150.86581.10080.12750.078*C160.59135 (18)0.91052 (8)0.05248 (16)0.0576 (5)H16A0.59820.95270.06690.069*H16B0.49000.89950.02260.069*C170.64489 (18)0.89559 (9)?0.05152 (17)0.0588 (5)H170.62230.8546?0.07970.071*C180.58172 (18)0.93738 (8)?0.16582 (17)0.0617 (5)H18A0.56280.9177?0.24740.074*H18B0.49350.9560?0.16950.074*C190.70447 (18)0.98060 (8)?0.13153 (16)0.0553 (4)C200.69973 (18)1.03873 (8)?0.18912 (16)0.0546 (4)C210.5711 (2)1.06028 (9)?0.28290 (18)0.0640 (5)H210.48821.0370?0.31200.077*C220.5655 (2)1.11605 (9)?0.33315 (19)0.0701 (5)H220.47921.1305?0.39550.084*C230.6886 (2)1.15008 (8)?0.2904 (2)0.0662 (5)C240.8184 (2)1.12962 (10)?0.1991 (2)0.0727 (6)H240.90111.1530?0.17180.087*C250.8234 (2)1.07410 (9)?0.14903 Iressa (19)0.0655 (5)H250.91061.0599?0.08750.079*C260.7429 (2)0.74050 (9)0.3414 (2)0.0749 (6)H26A0.64420.72700.31760.090*H26B0.79230.73850.43510.090*C270.8169 (2)0.70030 (9)0.2829 (2)0.0776 (6)H270.82220.66080.30620.093*C280.8743 (3)0.71473 (12)0.2031 (3)0.0922 (7)H28A0.87180.75370.17680.111*H28B0.91820.68620.17200.111*N10.67395 (14)0.88059 (7)0.17487 (13)0.0554 (4)N20.73969 (16)0.80148 (7)0.30080 (15)0.0633 (4)N30.82302 (15)0.96221 (7)?0.04143 (14)0.0606 (4)N40.6801 (3)1.20974 Iressa (9)?0.3438 (2)0.0907 (6)O10.52115 (15)0.79872 (6)0.12021 (14)0.0768 (4)O20.73990 (14)1.01619 (6)0.18463 (13)0.0677 (4)O31.27476 (15)0.97262 (6)0.53085 (13)0.0835 (4)O40.80057 (12)0.90603 (6)0.00001 (12)0.0663 (4)O50.5638 (2)1.22624 (8)?0.4262 (2)0.1111 (6)O60.7864 (2)1.24061 (9)?0.3026 (3)0.1445 (9) Notice in another window Atomic displacement guidelines (?2) U11U22U33U12U13U23C10.0496 (11)0.0657 (13)0.0690 (12)?0.0039 (10)0.0245 (10)?0.0025 (10)C20.0513 (11)0.0581 (11)0.0572 (10)?0.0025 (9)0.0231 (9)?0.0016 (8)C30.0439 (10)0.0582 (11)0.0491 (9)0.0041 (8)0.0193 (8)?0.0003 (8)C40.0464 (10)0.0516 (10)0.0463 (9)0.0034 (8)0.0204 (8)?0.0033 (7)C50.0488 (10)0.0559.